The Instrumentation Center


Select published research utilizing ICenter instrumentation:        (2010-2015)
  • Gold-Catalyzed Transannular [4+3] Cycloaddition Reactions, Benjamin W. Gung, Derek T. Craft, Lauren N. Bailey, Kristin Kirschbaum, Chemistry – A European Journal, 2010, 16, 639 – 644.
  • Relative substituent position on the strength of π–π stacking interactions, Benjamin W. Gung , Bright U. Emenike, Celeste N. Alverez, John Rakovan, Kristin Kirschbaum, Nirbhay Jain, Tetrahedron Letters, 2010, 51, 1648–1650.
  • Luminescent Low Valent Rhenium Complexes with 1,2-Bis(alkylphosphino)ethane Ligands.  Synthesis and X-ray Crystallographic, Electrochemical and Spectroscopic Characterization, Messersmith, Stephania J.; Kirschbaum, Kristin; Kirchhoff, Jon R., Inorganic Chemistry 2010, 49, 3857-3865.
  •  N,N'-Diethyl-4-nitrobenzene-1,3-diamine, 2,6-bis(ethylamino)-3-nitrobenzonitrile, and bis(4-ethylamino-3-  nitrophenyl)sulfone, Thomas J. Payne, Chad R. Thurman, Hao Yu, Qian Sun, Dillip K. Mohanty, Philip J. Squattrito*, Mark-Robin  Giolando, Christopher R. Brue,  Kristin Kirschbaum, Acta Cryst. 2010, C66, o369-o373
  •  Preparation and Characterization of Two New N-Heterocyclic Carbene Gold(I) Complexes and Comparison of Their Catalytic Activity to  Au(IPr)Cl, Benjamin W. Gung, Derek T. Craft, Lauren N. Bailey, Kristin Kirschbaum, Organometallics  2010,29, 3450-3456
  • Quantification of CH-π Interactions: Implications on How Substituent Effects Influence Aromatic Interactions, Benjamin W. Gung, Bright  U. Emenike, Michael Lewis, Kristin Kirschbaum, Chemistry – A European Journal 201016, 12352-12362
  • Confirmation of Bridging N-Indolides in 3-Methylindole and Di- and Tri(3-methylindolyl)methane Complexes of Dimethyl-, Diethyl-, and Di-iso-butylaluminum, Nicholas B. Kingsley, Kristin Kirschbaum, and Mark R. Mason, Organometallics 2010, 28, 5927-5935
  • Planar, Three-Coordinate Boron Monohydrides Ligated by Bis(3-methylindolyl)methanes, BingXu Song, Kristin Kirschbaum, Mark  R. Mason, Organometallics, 2012, 31,191-196
  • Synthesis and Calorimetric, Spectroscopic, and Structural Characterization of Isocyanide Complexes of Trialkylaluminum and Tri-tert-butylgallium, Nicholas B. Kingsley, Kristin Kirschbaum, Joseph A.Teprovich, Jr., Robert A. Flowers II, Mark R. Mason, Inorg. Chem., 2012, 51, 2494-2502
  • Electron Paramagnetic Resonance Spectroscopic Study of Copper Hopping in Doped bis(L-histidinato)Cadmium Dihydrate, Colaneri, Michael, Vitali, Jacqueline, Kirschbaum, Kristin, J. Phys. Chem. A, 2013, 117, 3414–3427
  • Ultrastable silver nanoparticles, Desireddy, Anil;Conn, Brian E,; Guo, Jingshu; Yoon, Bokwon; Barnett, Robert N.; Monahan, Bradley M.; Kirschbaum, Kristin; Griffith, Wendell P.; Whetten, Robert L.; Landman, Uzi; Bigioni, Terry P., Nature, 2013, 501, 399–402
  • A series of N-(2-phenylethyl) nitroaniline derivatives as precursors for slow and sustained nitric oxide release agents, Wade, Colin B.; Mohanty, Dillip K.; Squattrito, Philip J.; Amato, Nicholas J.;  Kirschbaum, Kristin, Acta Cryst., 2013, C69, 1383-1389
  • Bio-Based Bisfuran: Synthesis, Crystal Structure and  Low Molecular Weight Amorphous Polyester, Gaitonde Vishwanath; Lee Kyunghee; Kirschbaum Kristin; Sucheck Steven, Tetrahedron Letters, 2014; 55, 4141–4145.
  • Mono- and Bimetallic Aluminum Alkyl, Aryl, and Hydride Complexes of a Bulky Dipyrromethene Ligand, Gianopoulos, Christopher; Kirschbaum, Kristin; Mason, Mark R., Organometallics2014, 33, 4503–4511
  • Synthesis, Characterization and Crystal Structures of Mono and Dinuclear Macrocyclic Cobalt(II) Complexes with a new tetraaza m-xylyl-based macrocyclic ligand, Khandar, Ali Akbar; Kirschbaum,Kristin; Abedi, Marjan; Mock, Kristi; Tracy, Greg;  V. Spasojevic,V.; Hosseini-Yazdi,Seyed Abolfazl, New Journal of Chemistry, 2015, 39, 2822.
  • Structural patterns at all scales in a nonmetallic chiral Au133(SR)52 nanoparticle, Chenjie Zeng, Yuxiang Chen, Kristin Kirschbaum, Kannatassen Appavoo, Matthew Y. Sfeir, and Rongchao Jin, Science Advances, 2015, 1, e1500045, 
  • P. Langan, A. K. Sangha, T. Wymore, J. M. Parks, Z. K. Yang, L. Hanson, Z. Fisher, S. A. Mason, M. P. Blakeley, T. Forsyth, J. P. Glusker, H. L. Carrell, J. C. Smith, D. A. Keen, D. E. Graham, & A. Kovalevsky
 (2014) L-Arabinose Binding, Isomerization, and Epimerization by D-Xylose Isomerase: X-Ray/Neutron Crystallographic and Molecular Simulation Study. Structure, 22, 1287–1300.
  • Sawada, D., Hanson, L., Wada, M., Nishiyama, Y., & Langan, P. (2014) The initial structure of cellulose during ammonia pretreatment. Cellulose 21, 1117-1126.
  • Langan, P., Petridis, L., O’Neill, H.M., Pingali, S.V., Foston, M., Nishiyama, Y., Schultz, R., Lindner, B., Hanson, B.L., Harton, S., Heller, W.T., Urban, V., Evans, B.R., Gnaankaran, S., Ragauskas, A.J., Smith, J.C. &Davison, B. (2014) Common processes drive the thermochemical pretreatment of lignocellulosic biomass. Green Chemistry 16, 63-68.
  • Barr, C.J., Hanson, B.L., Click, K., Perotta, G., & Schall, C.A. (2014) Influence of ionic-liquid incubation temperature on changes in cellulose structure, biomass composition, and enzymatic digestibility. Cellulose 21,973-982.
  • Chen, J.C.H., Hanson, B.L., Fisher, S.Z., Langan, P.A., & Kovalevsky, A.Y. (2012) Direct observation of hydrogen atom dynamics and interactions by ultra-high resolution neutron protein crystallography. Proc. Natl. Acad. Sci. USA, 109, 15301-15306.
  • Kovalevsky, A. Y., Hanson, B. L., Mason, S. A., Forsyth, V. T., Fisher, Z., Mustyakimov, M., Blakeley, M. P., Keen, D. A. & Langan, P. (2012) Inhibition of D-xylose isomerase by polyols: atomic details by joint X-ray/neutron crystallography. Acta Cryst. D68, 1201-1206.
  • Kovalevsky, A. Y., Johnson, H., Hanson, B. L., Waltman, M. J., Fisher, S. Z., Taylor, S. & Langan, P. (2012) Low- and room-temperature X-ray structures of protein kinase A ternary complexes shed new light on its activity. Acta Cryst. D68, 854-860.
  • I. P. Samayam, B. L. Hanson. P. Langan & C. A. Schall (2011) Ionic-Liquid Induced Changes in Cellulose Structure Associated with Enhance Biomass Hydrolysis.  Biomacromolecules 12, 3091-3098.
  • A. Y. KovalevskyB. L. Hanson, S. A. Mason, T. Yoshida, S. Z. Fisher, M. Mustyakimov, V. T. Forsyth, M. P. Blakeley, D. A. Keen & P. Langan (2011) Identification of the Elusive Hydronium Ion Exchanging Roles with a Proton in an Enzyme at Lower pH Values. Angewandte Chemie 50, 7520-7523.
  • B. N. Shah, U. Chinte, S. J. Tomanicek, B. L Hanson, & Constance A. Schall (2011) Flash Cooling Protein Crystals: Estimate of Cryoprotectant Concentration Using Thermal Properties. Crystal Growth & Design 11, 1493-1501.
  • A. Y. KovalevskyB. L. HansonS. SeaverS. Z. FisherM. Mustyakimov & P. Langan (2011) Preliminary joint X-ray and neutron protein crystallographic studies of endoxylanase II from the fungus Trichoderma longibrachiatumActa CrystF67, 283-286.
  • M. Lucas, G. L. Wagner, Y. Nishiyama, L. Hanson, I. P. Samayam, C. A. Schall, P. Langan & K. D. Rector (2011) Reversible swelling of the cell wall of poplar biomass by ionic liquid at room temperature.  Bioresource Technology 102, 4518-4523.
  • M.-M. BlumS. J. TomanicekH. JohnB. L. HansonH. RüterjansB. P. SchoenbornP. Langan & J. C.-H. Chen (2010). X-ray structure of perdeuterated diisopropyl fluorophosphatase (DFPase): perdeuteration of proteins for neutron diffraction. Acta Cryst. F66, 379-385.
  • A. Y. KovalevskyS. Z. FisherS. SeaverM. MustyakimovN. SukumarP. LanganT. C. Mueser & B. L. Hanson (2010). Preliminary neutron and X-ray crystallographic studies of equine cyanomethemoglobin. Acta Cryst. F66, 474-477.
  • T. C. MueserW. P. GriffithA. Y. KovalevskyJ. GuoS. SeaverP. Langan & B. L. Hanson (2010). Hemoglobin redux: combining neutron and X-ray diffraction with mass spectrometry to analyse the quaternary state of oxidized hemoglobins. Acta Cryst. D66, 1249-1256
  • J. P. GluskerH. L. CarrellA. Y. KovalevskyL. HansonS. Z. FisherM. MustyakimovS. MasonT. Forsyth & P. Langan (2010). Using neutron protein crystallography to understand enzyme mechanisms. Acta Cryst. D66, 1257-1261.
  • Kovalevsky AYHanson LFisher SZMustyakimov MMason SAForsyth VTBlakeley MPKeen DAWagner TCarrell HLKatz AKGlusker JPLangan P. (2010) Metal ion roles and the movement of hydrogen during reaction catalyzed by D-xylose isomerase: a joint x-ray and neutron diffraction study.Structure.18(6):688-699
  • Yoshiharu NishiyamaMasahisa WadaB. Leif Hanson and Paul Langan (2010) Time-resolved X-ray diffraction microprobe studies of the conversion of cellulose I to ethylenediamine-cellulose I. Cellulose 17, 735-745.
Last Updated: 6/9/16